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Fast side reactions under the conditions of acid-catalyzed alkylation are oligomerization (polymerization) and conjunct polymerization The latter involves polymerization, isomerization, cyclization, and hydrogen transfer to yield cyclic polyalkapolyenes To suppress these side reactions, relatively high (10: 1) alkane: alkene ratios are usually applied in commercial alkylations Sulfuric acid and anhydrous hydrogen fluoride are most widely used in industrial alkene-isoalkane alkylations The former results in significant amounts of acidsoluble oil formation, which together with the more difficult acid regeneration led to wider use of the hydrogen fluoride alkylation Environmental considerations of the effect of the toxicity of volatile HF if accidentally released into the atmosphere necessitated development of modified HF alkylation For example, relatively stable (and therefore less volatile) environmentally safe onium polyhydrogen fluoride complexes, such as pyridine-(HF)x complexes, are used for alkylation (see Section 551).

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Future generation of catalysts probably will be solids, but their use will necessitate higher temperatures with associated difficulties, and large capital investment is needed to start new plants Zeolites tend to lose their catalytic activity during alkylation and give rather complex product distribution The latter originates, in part, from the strong adsorption of hydrocarbons resulting in alkane self-alkylation and extensive cracking Furthermore, preferential adsorption of alkenes can bring about oligomerization Despite these difficulties, the alkylate produced on zeolites (and other solid catalysts) is very similar to that formed in liquid-phase alkylation In both cases trimethylpentanes are the main products and isopentane is always present This suggests that the carbocationic mechanism discussed above is also operative with zeolites and other solid acid catalysts.

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</antcall> <mkdir dir= ${build.destdir}/${ejbpkg}/META-INF /> <copy todir= ${build.destdir}/${ejbpkg}/META-INF > <fileset dir= ${src.dir}/subject/invoice/${ejbpkg}/META-INF includes= **/* /> </copy> <jar destfile= ${build.destdir}/${ejbpkg}.jar manifest= config/${ejbpkg}.mf basedir= ${build.destdir}/${ejbpkg} /> </target> <target name= _internal.compile > <mkdir dir= ${build.destdir} /> <javac srcdir= ${src.dir} compiler= modern destdir= ${build.destdir} deprecation= ${javac.deprecation} debug= ${javac.debug} verbose= off includes= ${included.files} > <classpath refid= classpath /> <classpath path= ${classpath.extras} /> </javac> </target>

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New types of solid acid catalysts (H3P04-BF3-H2S04 supported on Si02 or Zr02) were reported to exhibit only small deactivation in the isobutane-butene reaction 6 H2S04 was shown to bring about a remarkable increase in the number of acid sites, whereas BF3 enhances acid strength..

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